JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001730
Submitter
The Noguchi Institute
Reaction ID
R-0000-001730
Regist Date
2012/06/21 17:45:35
REACTANT
MOLECULE ID
JCGG-COM0002255 (Reaction Tree)
Mol
0.3 mmol
MOLECULE ID
JCGG-COM0000810
Reactant Type
DAST
Mol
0.46 mmol
MOLECULE ID
JCGG-COM0000603
Reactant Type
NBS
Mol
0.39 mmol
PRODUCT
MOLECULE ID
JCGG-COM0002256 (Reaction Tree)
Yield
85%
REACTION DETAIL
Reaction Time
2 + 25 minutes
Reaction Temp
-15 degree C
Solvent
CH2Cl2
Comment
NBS was added 2 minutes after the initiation of the reaction.
COMMENT
Keywords: glycosyl fluorides, glycosyl sulfides, hexasaccharide
ATTENTION: The reference is wrong.
REFERENCE
Reference Id
REF-0000-000196
Source
PREPARATIVE CARBOHYDRATE CHEMISTRY
Reference Id
REF-0000-000197
Source
ISBN 0-8247-9802-3
Reference Id
REF-0000-000226
Source
unknown

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