JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001725
Submitter
The Noguchi Institute
Reaction ID
R-0000-001725
Regist Date
2012/06/21 17:44:50
REACTANT
MOLECULE ID
JCGG-COM0002246 (Reaction Tree)
Skeleton
JCGG-STR031569
Mol
1.0 mmol
MOLECULE ID
JCGG-COM0000552
Reactant Type
HCl
Mol
saturated
PRODUCT
MOLECULE ID
JCGG-COM0002247 (Reaction Tree)
Skeleton
JCGG-STR032525
Yield
78%
REACTION DETAIL
Reaction Time
4 hours
Reaction Temp
room temp
Solvent
dry CH2Cl2
COMMENT
Keywords: glycosylation, O-glycosyl trichloroacetimidates
5% of alpha-halogenose was also obtained.
REFERENCE
Reference Id
REF-0000-000196
Source
PREPARATIVE CARBOHYDRATE CHEMISTRY
Reference Id
REF-0000-000197
Source
ISBN 0-8247-9802-3
Reference Id
REF-0000-000223
Source
Liebigs Ann. Chem. p. 680 (1984)

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)