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Glycan Syntheses |
JCGG ID |
JCGG-RAC0001722 | ||||
Submitter |
The Noguchi Institute | ||||
Reaction ID |
R-0000-001722
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Regist Date |
2012/06/21 17:44:17 | ||||
| REACTANT | |||||
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Mol |
0.6 mmol | ||||
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Mol |
0.8 mmol | ||||
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Reactant Type |
TMSOTf (0.1 M in CH2Cl2) | ||||
Mol |
0.03 mmol | ||||
| PRODUCT | |||||
MOLECULE ID |
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Yield |
68% | ||||
| REACTION DETAIL | |||||
Reaction Time |
2 hours | ||||
Reaction Temp |
room temp | ||||
Solvent |
CH2Cl2 | ||||
Comment |
TMSOTf was added slowly. | ||||
| COMMENT | |||||
| Keywords: glycosylation, O-glycosyl trichloroacetimidates | |||||
| REFERENCE | |||||
Reference Id |
REF-0000-000196 | ||||
Source |
PREPARATIVE CARBOHYDRATE CHEMISTRY | ||||
Reference Id |
REF-0000-000197 | ||||
Source |
ISBN 0-8247-9802-3 | ||||
Reference Id |
REF-0000-000221 | ||||
Source |
Carbohydr. Res. 269:217 (1995) | ||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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