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Glycan Syntheses |
JCGG ID |
JCGG-RAC0001720 | ||||
Submitter |
The Noguchi Institute | ||||
Reaction ID |
R-0000-001720
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Regist Date |
2012/06/21 17:43:38 | ||||
| REACTANT | |||||
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Mol |
0.076 mmol | ||||
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Mol |
0.15 mmol | ||||
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Reactant Type |
BF3*OEt2 | ||||
Mol |
0.16 micro mole | ||||
| PRODUCT | |||||
MOLECULE ID |
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Yield |
60% | ||||
| REACTION DETAIL | |||||
Reaction Time |
6 hours | ||||
Reaction Temp |
-20 degree C | ||||
Solvent |
dry CH2Cl2 | ||||
Comment |
48, 49, and MS 4A were mixed and stirred for 6 hours at room temperature before the reaction. | ||||
| MS 4A was included in the solvent. | |||||
| COMMENT | |||||
| Keywords: glycosylation, O-glycosyl trichloroacetimidates | |||||
| REFERENCE | |||||
Reference Id |
REF-0000-000196 | ||||
Source |
PREPARATIVE CARBOHYDRATE CHEMISTRY | ||||
Reference Id |
REF-0000-000197 | ||||
Source |
ISBN 0-8247-9802-3 | ||||
Reference Id |
REF-0000-000219 | ||||
Source |
Carbohydr. Res. 246:75 (1993) | ||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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