JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001709
Submitter
The Noguchi Institute
Reaction ID
R-0000-001709
Regist Date
2012/06/21 17:41:45
REACTANT
MOLECULE ID
JCGG-COM0002209 (Reaction Tree)
Mol
1.25 mmol
MOLECULE ID
JCGG-COM0002210 (Reaction Tree)
Skeleton
JCGG-STR025280
Mol
2.00 mmol
MOLECULE ID
JCGG-COM0000785
Reactant Type
Zn(OTf)2 (0.1 M in propionitrile)
Mol
12.5 micro mole
PRODUCT
MOLECULE ID
JCGG-COM0002211 (Reaction Tree)
Yield
71%
REACTION DETAIL
Reaction Time
30 minutes
Reaction Temp
room temp
Solvent
dry propionitrile
COMMENT
Keywords: glycosylation, O-glycosyl trichloroacetimidates
REFERENCE
Reference Id
REF-0000-000196
Source
PREPARATIVE CARBOHYDRATE CHEMISTRY
Reference Id
REF-0000-000197
Source
ISBN 0-8247-9802-3
Reference Id
REF-0000-000209
Source
T. Stauch, Dissertation, Universitat Konstanz, 1995

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)