JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001708
Submitter
The Noguchi Institute
Reaction ID
R-0000-001708
Regist Date
2012/06/21 17:41:28
REACTANT
MOLECULE ID
JCGG-COM0002206 (Reaction Tree)
Mol
4.0 mmol
MOLECULE ID
JCGG-COM0002207 (Reaction Tree)
Mol
4.5 mmol
MOLECULE ID
JCGG-COM0000009
Reactant Type
TMSOTf (0.05 M)
Mol
40 micro mole
PRODUCT
MOLECULE ID
JCGG-COM0002208 (Reaction Tree)
Yield
80%
REACTION DETAIL
Reaction Time
10 minutes
Reaction Temp
-40 degree C
Solvent
dry MeCN
COMMENT
Keywords: glycosylation, O-glycosyl trichloroacetimidates
REFERENCE
Reference Id
REF-0000-000196
Source
PREPARATIVE CARBOHYDRATE CHEMISTRY
Reference Id
REF-0000-000197
Source
ISBN 0-8247-9802-3
Reference Id
REF-0000-000208
Source
Liebigs Ann. Chem. p. 449 (1994)

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)