|
Glycan Syntheses |
JCGG ID |
JCGG-RAC0001705 | ||||
Submitter |
The Noguchi Institute | ||||
Reaction ID |
R-0000-001705
|
||||
Regist Date |
2012/06/21 17:40:25 | ||||
| REACTANT | |||||
|
|
|
||||
Mol |
2.67 mmol | ||||
|
|
|
||||
Reactant Type |
CCl3CN | ||||
Mol |
138 mmol | ||||
|
|
|
||||
Reactant Type |
DBU | ||||
Volume |
5 drops | ||||
| PRODUCT | |||||
MOLECULE ID |
|
|
|||
Product Type |
alpha | ||||
Yield |
100%(alpha/beta=1/2) | ||||
MOLECULE ID |
|
|
|||
Product Type |
beta | ||||
Yield |
100%(alpha/beta=1/2) | ||||
| REACTION DETAIL | |||||
Reaction Time |
30 minutes | ||||
Reaction Temp |
NOT specified | ||||
Solvent |
dry CH2Cl2 | ||||
| COMMENT | |||||
| Keywords: synthesis, O-glycosyl trichloroacetimidates | |||||
| REFERENCE | |||||
Reference Id |
REF-0000-000196 | ||||
Source |
PREPARATIVE CARBOHYDRATE CHEMISTRY | ||||
Reference Id |
REF-0000-000197 | ||||
Source |
ISBN 0-8247-9802-3 | ||||
Reference Id |
REF-0000-000208 | ||||
Source |
Liebigs Ann. Chem. p. 449 (1994) | ||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
|