JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001702
Submitter
The Noguchi Institute
Reaction ID
R-0000-001702
Regist Date
2012/06/21 17:39:18
REACTANT
MOLECULE ID
JCGG-COM0002191 (Reaction Tree)
Mol
8.61 mmol
MOLECULE ID
JCGG-COM0000521
Reactant Type
CCl3CN
Mol
24.8 mmol
MOLECULE ID
JCGG-COM0000842
Reactant Type
K2CO3
Weight
2 g
PRODUCT
MOLECULE ID
JCGG-COM0002192 (Reaction Tree)
Skeleton
JCGG-STR031569
Yield
54%
REACTION DETAIL
Reaction Time
2 hours
Reaction Temp
room temp
Solvent
dry CH2Cl2
COMMENT
Keywords: synthesis, O-glycosyl trichloroacetimidates
REFERENCE
Reference Id
REF-0000-000196
Source
PREPARATIVE CARBOHYDRATE CHEMISTRY
Reference Id
REF-0000-000197
Source
ISBN 0-8247-9802-3
Reference Id
REF-0000-000205
Source
Liebigs Ann. Chem. p. 1343 (1984)

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)