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Glycan Syntheses |
JCGG ID |
JCGG-RAC0001700 | ||||
Submitter |
The Noguchi Institute | ||||
Reaction ID |
R-0000-001700
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Regist Date |
2012/06/21 17:39:06 | ||||
| REACTANT | |||||
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Mol |
0.653 to 0.907 mmol | ||||
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Reactant Type |
pyridine (solvent) | ||||
Volume |
33.3 mL | ||||
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Reactant Type |
Ac2O (solvent) | ||||
Volume |
16.7 mL | ||||
| PRODUCT | |||||
MOLECULE ID |
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Yield |
72%(at least) | ||||
| REACTION DETAIL | |||||
Reaction Time |
18 hours | ||||
Reaction Temp |
NOT specified | ||||
Solvent |
pyridine/Ac2O = 2/1 | ||||
| COMMENT | |||||
| Keywords: O-glycopeptide, N-glycopeptide, synthesis, selectively deprotected building blocks, stability against acids | |||||
| REFERENCE | |||||
Reference Id |
REF-0000-000196 | ||||
Source |
PREPARATIVE CARBOHYDRATE CHEMISTRY | ||||
Reference Id |
REF-0000-000197 | ||||
Source |
ISBN 0-8247-9802-3 | ||||
Reference Id |
REF-0000-000201 | ||||
Source |
Angew. Chem. Int. Ed. Engl. 27:1697 (1988) | ||||
Reference Id |
REF-0000-000203 | ||||
Source |
Bioorg. Med. Chem. 2:1189 (1994) | ||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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