JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001700
Submitter
The Noguchi Institute
Reaction ID
R-0000-001700
Regist Date
2012/06/21 17:39:06
REACTANT
MOLECULE ID
JCGG-COM0002188 (Reaction Tree)
Mol
0.653 to 0.907 mmol
MOLECULE ID
JCGG-COM0000979
Reactant Type
pyridine (solvent)
Volume
33.3 mL
MOLECULE ID
JCGG-COM0000086
Reactant Type
Ac2O (solvent)
Volume
16.7 mL
PRODUCT
MOLECULE ID
JCGG-COM0002189 (Reaction Tree)
Yield
72%(at least)
REACTION DETAIL
Reaction Time
18 hours
Reaction Temp
NOT specified
Solvent
pyridine/Ac2O = 2/1
COMMENT
Keywords: O-glycopeptide, N-glycopeptide, synthesis, selectively deprotected building blocks, stability against acids
REFERENCE
Reference Id
REF-0000-000196
Source
PREPARATIVE CARBOHYDRATE CHEMISTRY
Reference Id
REF-0000-000197
Source
ISBN 0-8247-9802-3
Reference Id
REF-0000-000201
Source
Angew. Chem. Int. Ed. Engl. 27:1697 (1988)
Reference Id
REF-0000-000203
Source
Bioorg. Med. Chem. 2:1189 (1994)

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)