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Glycan Syntheses |
JCGG ID |
JCGG-RAC0001692 | |||||||
Submitter |
The Noguchi Institute | |||||||
Reaction ID |
R-0000-001692
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Regist Date |
2012/06/21 17:37:54 | |||||||
| REACTANT | ||||||||
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Mol |
2.8 mmol | |||||||
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|
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|||||||
Reactant Type |
N-methyl aniline | |||||||
Volume |
0.5 mL | |||||||
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|||||||
Reactant Type |
[(C6H5)3P]4Pd (50 mg, 1.5 mol%) | |||||||
Mol |
0.043 mmol | |||||||
| PRODUCT | ||||||||
MOLECULE ID |
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Yield |
96% | |||||||
| REACTION DETAIL | ||||||||
Reaction Time |
2 hours | |||||||
Reaction Temp |
NOT specified | |||||||
Solvent |
dry THF | |||||||
Comment |
The reaction was conducted in dark condition. | |||||||
| COMMENT | ||||||||
| Keywords: O-glycopeptide, N-glycopeptide, synthesis, selectively deprotected building blocks, allyl ester protecting group | ||||||||
| REFERENCE | ||||||||
Reference Id |
REF-0000-000196 | |||||||
Source |
PREPARATIVE CARBOHYDRATE CHEMISTRY | |||||||
Reference Id |
REF-0000-000197 | |||||||
Source |
ISBN 0-8247-9802-3 | |||||||
Reference Id |
REF-0000-000200 | |||||||
Source |
Synlett p. 593 (1991) | |||||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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