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Glycan Syntheses |
JCGG ID |
JCGG-RAC0001690 | |||||||
Submitter |
The Noguchi Institute | |||||||
Reaction ID |
R-0000-001690
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Regist Date |
2012/06/21 17:37:43 | |||||||
| REACTANT | ||||||||
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Mol |
5.8 mmol | |||||||
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Reactant Type |
AcOH | |||||||
Volume |
1 mL | |||||||
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Reactant Type |
(C8H17)3P (in 10 mL of THF) | |||||||
Mol |
7.4 mmol | |||||||
| PRODUCT | ||||||||
MOLECULE ID |
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Yield |
94% | |||||||
| REACTION DETAIL | ||||||||
Reaction Time |
2 hours | |||||||
Reaction Temp |
0 degree C | |||||||
Solvent |
dry THF | |||||||
Comment |
The addition of AcOH was performed before the addition of (C8H17)3P. | |||||||
| COMMENT | ||||||||
| Keywords: O-glycopeptide, N-glycopeptide, synthesis, selectively deprotected building blocks, allyl ester protecting group | ||||||||
| REFERENCE | ||||||||
Reference Id |
REF-0000-000196 | |||||||
Source |
PREPARATIVE CARBOHYDRATE CHEMISTRY | |||||||
Reference Id |
REF-0000-000197 | |||||||
Source |
ISBN 0-8247-9802-3 | |||||||
Reference Id |
REF-0000-000200 | |||||||
Source |
Synlett p. 593 (1991) | |||||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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