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Glycan Syntheses |
JCGG ID |
JCGG-RAC0001688 | ||||
Submitter |
The Noguchi Institute | ||||
Reaction ID |
R-0000-001688
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Regist Date |
2012/06/21 17:37:29 | ||||
| REACTANT | |||||
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Reactant Type |
hydrochloride | ||||
Mol |
30.6 mmol | ||||
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Reactant Type |
FmocCl (in dioxane) | ||||
Mol |
41.8 mmol | ||||
| PRODUCT | |||||
MOLECULE ID |
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Yield |
96% | ||||
| REACTION DETAIL | |||||
Reaction Time |
24 hours | ||||
Reaction Temp |
0 degree C | ||||
Solvent |
saturated NaHCO3 solution and dioxane | ||||
Comment |
The hydrochloride was added dropwise. | ||||
| COMMENT | |||||
| Keywords: O-glycopeptide, N-glycopeptide, synthesis, selectively deprotected building blocks, allyl ester protecting group | |||||
| REFERENCE | |||||
Reference Id |
REF-0000-000196 | ||||
Source |
PREPARATIVE CARBOHYDRATE CHEMISTRY | ||||
Reference Id |
REF-0000-000197 | ||||
Source |
ISBN 0-8247-9802-3 | ||||
Reference Id |
REF-0000-000200 | ||||
Source |
Synlett p. 593 (1991) | ||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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