JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001682
Submitter
The Noguchi Institute
Reaction ID
R-0000-001682
Regist Date
2012/06/21 17:36:43
REACTANT
MOLECULE ID
JCGG-COM0002153 (Reaction Tree)
Skeleton
JCGG-STR031571
Mol
1 mmol
MOLECULE ID
JCGG-COM0001032
Reactant Type
morpholine (may be mixed with CH2Cl2)
Volume
10 mL
PRODUCT
MOLECULE ID
JCGG-COM0002154 (Reaction Tree)
Skeleton
JCGG-STR031571
Yield
98%
REACTION DETAIL
Reaction Time
30 minutes
Reaction Temp
NOT specified
Solvent
morpholine (+CH2Cl2)
COMMENT
Keywords: O-glycopeptide, N-glycopeptide, synthesis, selectively deprotected building blocks, fluorenylmethoxycarbonyl group, Fmoc, benzyl esters
The reaction is the 2nd part of the sequence.
REFERENCE
Reference Id
REF-0000-000196
Source
PREPARATIVE CARBOHYDRATE CHEMISTRY
Reference Id
REF-0000-000197
Source
ISBN 0-8247-9802-3
Reference Id
REF-0000-000198
Source
Angew. Chem. Int. Ed. Engl. 22:62 (1983)

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)