JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001680
Submitter
The Noguchi Institute
Reaction ID
R-0000-001680
Regist Date
2012/06/21 17:36:27
REACTANT
MOLECULE ID
JCGG-COM0002149 (Reaction Tree)
Skeleton
JCGG-STR031571
Mol
0.4 mmol
MOLECULE ID
JCGG-COM0000489
Reactant Type
hydrazine hydrate (100%)
Volume
20 mL
PRODUCT
MOLECULE ID
JCGG-COM0002150 (Reaction Tree)
Skeleton
JCGG-STR031571
Yield
86%
REACTION DETAIL
Reaction Time
40 minutes
Reaction Temp
room temp
Solvent
MeOH
COMMENT
Keywords: O-glycopeptide, N-glycopeptide, synthesis, selectively deprotected building blocks, fluorenylmethoxycarbonyl group, Fmoc, benzyl esters
REFERENCE
Reference Id
REF-0000-000196
Source
PREPARATIVE CARBOHYDRATE CHEMISTRY
Reference Id
REF-0000-000197
Source
ISBN 0-8247-9802-3
Reference Id
REF-0000-000198
Source
Angew. Chem. Int. Ed. Engl. 22:62 (1983)

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)