JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001659
Submitter
The Noguchi Institute
Reaction ID
R-0000-001659
Regist Date
2012/06/21 17:33:17
REACTANT
MOLECULE ID
JCGG-COM0002119 (Reaction Tree)
MOLECULE ID
JCGG-COM0001653
Reactant Type
TiBr4
PRODUCT
MOLECULE ID
JCGG-COM0002120 (Reaction Tree)
Yield
97%
REACTION DETAIL
Reaction Time
6 hours
Reaction Temp
20 degree C
Solvent
CH2Cl2
Comment
Very few were described regarding this reaction.
COMMENT
Keywords: synthesis of glycopeptide, O-glycan
The reaction is the 2nd part of the sequence.
REFERENCE
Reference Id
REF-0000-000073
Source
第4版 実験化学講座 (26), 丸善
Reference Id
REF-0000-000074
Source
ISBN 4-621-03702-1
Reference Id
REF-0000-000194
Source
H. Paulsen and M. Paal, Carbohydr. Res., 135, 53 (1984) ; H. Paulsen and M. Paal, ibid., 135, 71 (1984)

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)