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Glycan Syntheses |
JCGG ID |
JCGG-RAC0001607 | ||||
Submitter |
The Noguchi Institute | ||||
Reaction ID |
R-0000-001607
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Regist Date |
2012/06/21 17:25:27 | ||||
| REACTANT | |||||
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Mol |
1.94 mmol | ||||
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Reactant Type |
HO(CH2)8COOMe | ||||
Mol |
2.92 mmol | ||||
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Reactant Type |
BF3*OEt2 (in 7.0 mL of ClCH2CH2Cl/hexane) | ||||
Mol |
1.06 mmol | ||||
| PRODUCT | |||||
MOLECULE ID |
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Yield |
33% | ||||
| REACTION DETAIL | |||||
Reaction Time |
30 minutes | ||||
Reaction Temp |
-40 degree C | ||||
Solvent |
ClCH2CH2Cl/hexane = 1/1 | ||||
Comment |
2, HO(CH2)8COOMe, and MS 4A were mixed and stirred for 1 hour at before the reaction. | ||||
| MS 4A was included in the solvent. | |||||
| BF3*OEt2 was added dropwise. | |||||
| COMMENT | |||||
| Keywords: biological activity, carbohydrates, conformation analysis, lectins, synthesis design | |||||
| REFERENCE | |||||
Reference Id |
REF-0000-000189 | ||||
Issn |
|||||
Doi |
10.1002/chem.200400831 | ||||
PubMed ID |
15770712 | ||||
Journal Name |
Chemistry (Weinheim an der Bergstrasse, Germany). (2005) 11 (10): 3032-8. | ||||
Article Title |
Synthesis and evaluation of 5-thio-L-fucose-containing oligosaccharide. | ||||
Author |
Masayuki, Izumi; Osamu, Tsuruta; Yasuhiro, Kajihara; Shin, Yazawa; Hideya, Yuasa; Hironobu, Hashimoto | ||||
Affiliation |
Department of Life Science, Graduate school of Bioscience and Biotechnology, Tokyo Institute of Technology, 4259 Nagatsuta, Yokohama 226-8501, Japan.masayuki.izumi@aist.go.jp | ||||
Reference Id |
REF-0000-000190 | ||||
Source |
Chem. Eur. J. 2005, 11, 3032-3038 | ||||
Doi |
10.1002/chem.200400831 | ||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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