JCGG ID |
JCGG-RAC0001569 | ||||
Submitter |
The Noguchi Institute | ||||
Reaction ID |
R-0000-001569 | ||||
Regist Date |
2012/06/21 17:22:17 | ||||
REACTANT | |||||
|
|
||||
Mol |
1.4 mmol | ||||
|
|
||||
Reactant Type |
anisoyl chloride | ||||
Mol |
4.29 mmol | ||||
PRODUCT | |||||
MOLECULE ID |
|
|
|||
Yield |
92% | ||||
REACTION DETAIL | |||||
Reaction Time |
15 minutes | ||||
Reaction Temp |
room temp | ||||
Solvent |
pyridine | ||||
Comment |
Anisoyl chloride was added dropwise. | ||||
COMMENT | |||||
Keywords: carbohydrates, glycosides, glycosylation, oligosaccharides, synthetic methods | |||||
ATTENTION: There is a typo in the written method. (compound 2b should be 1b) | |||||
REFERENCE | |||||
Reference Id |
REF-0000-000187 | ||||
Issn |
Electronic | ||||
Doi |
10.1002/anie.201007212 | ||||
PubMed ID |
21433229 | ||||
Journal Name |
Angewandte Chemie (International ed. in English). (2011) 50 (18): 4197-201. | ||||
Article Title |
S-Benzimidazolyl glycosides as a platform for oligosaccharide synthesis by an active-latent strategy. | ||||
Author |
Scott J, Hasty; Matthew A, Kleine; Alexei V, Demchenko | ||||
Affiliation |
Department of Chemistry and Biochemistry, University of Missouri-St.?Louis, One University Boulevard, St.?Louis, MO 63121, USA. | ||||
Reference Id |
REF-0000-000188 | ||||
Source |
Angew. Chem. Int. Ed. 2011, 50, 4197-4201 | ||||
Doi |
10.1002/anie.201007212 |
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST) |