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Glycan Syntheses |
JCGG ID |
JCGG-RAC0001562 | ||||
Submitter |
The Noguchi Institute | ||||
Reaction ID |
R-0000-001562
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Regist Date |
2012/06/21 17:21:29 | ||||
| REACTANT | |||||
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||||
Reactant Type |
bromide | ||||
Mol |
3.75 mmol | ||||
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||||
Reactant Type |
KSBiz | ||||
Mol |
9.36 mmol | ||||
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||||
Reactant Type |
18-crown-6 | ||||
Mol |
0.75 mmol | ||||
| PRODUCT | |||||
MOLECULE ID |
|
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Yield |
53% | ||||
| REACTION DETAIL | |||||
Reaction Time |
16 hours | ||||
Reaction Temp |
room temp | ||||
Solvent |
MeCN | ||||
Comment |
MS 3A was included in the solvent. | ||||
| COMMENT | |||||
| Keywords: carbohydrates, glycosides, glycosylation, oligosaccharides, synthetic methods | |||||
| REFERENCE | |||||
Reference Id |
REF-0000-000187 | ||||
Issn |
Electronic | ||||
Doi |
10.1002/anie.201007212 | ||||
PubMed ID |
21433229 | ||||
Journal Name |
Angewandte Chemie (International ed. in English). (2011) 50 (18): 4197-201. | ||||
Article Title |
S-Benzimidazolyl glycosides as a platform for oligosaccharide synthesis by an active-latent strategy. | ||||
Author |
Scott J, Hasty; Matthew A, Kleine; Alexei V, Demchenko | ||||
Affiliation |
Department of Chemistry and Biochemistry, University of Missouri-St.？Louis, One University Boulevard, St.？Louis, MO 63121, USA. | ||||
Reference Id |
REF-0000-000188 | ||||
Source |
Angew. Chem. Int. Ed. 2011, 50, 4197-4201 | ||||
Doi |
10.1002/anie.201007212 | ||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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