JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
 JCGG-RAC0001557
Submitter
 The Noguchi Institute
Reaction ID
 R-0000-001557
Regist Date
 2012/06/21 17:20:55
REACTANT
MOLECULE ID
 JCGG-COM0002003 (Reaction Tree)
Skeleton
JCGG-STR019256
MOLECULE ID
 JCGG-COM0000491
Reactant Type
 AcOH (70%)
PRODUCT
MOLECULE ID
 JCGG-COM0002004 (Reaction Tree)
Skeleton
JCGG-STR019256
Yield
 92%
REACTION DETAIL
Reaction Time
 3 to 4 hours
Reaction Temp
 70 degree C
Solvent
 AcOH
Comment
 Very few were described regarding this reaction.
COMMENT
Keywords: protection of sugar hydroxy groups, cycloacetal group protection
REFERENCE
Reference Id
 REF-0000-000073
Source
 第4版 実験化学講座 (26), 丸善
Reference Id
 REF-0000-000074
Source
 ISBN 4-621-03702-1
Reference Id
 REF-0000-000185
Source
 P. J. Garegg, S. Oscarson, and A.-K. Tiden, Carbohydr. Res., 200, 475 (1990)
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)