JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001556
Submitter
The Noguchi Institute
Reaction ID
R-0000-001556
Regist Date
2012/06/21 17:20:46
REACTANT
MOLECULE ID
JCGG-COM0002001 (Reaction Tree)
Skeleton
JCGG-STR001961
MOLECULE ID
JCGG-COM0000498
Reactant Type
p-TsOH
MOLECULE ID
JCGG-COM0000375
Reactant Type
Bn(OMe)2
PRODUCT
MOLECULE ID
JCGG-COM0002002 (Reaction Tree)
Skeleton
JCGG-STR001961
Yield
91%
REACTION DETAIL
Reaction Time
overnight
Reaction Temp
22 degree C
Solvent
MeCN
Comment
Very few were described regarding this reaction.
COMMENT
Keywords: protection of sugar hydroxy groups, cycloacetal group protection
REFERENCE
Reference Id
REF-0000-000073
Source
第4版 実験化学講座 (26), 丸善
Reference Id
REF-0000-000074
Source
ISBN 4-621-03702-1
Reference Id
REF-0000-000184
Source
K. Jansson, S. Ahlfors, T. Frejd, J. Kihlberg, and G. Magnusson, J. Org. Chem., 53, 5629 (1988)

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)