JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001545
Submitter
The Noguchi Institute
Reaction ID
R-0000-001545
Regist Date
2012/06/21 17:19:20
REACTANT
MOLECULE ID
JCGG-COM0001975 (Reaction Tree)
Skeleton
JCGG-STR004776
Mol
1 mmol
MOLECULE ID
JCGG-COM0000489
Reactant Type
NH2NH2*H2O (in 10 mL of pyridine/AcOH = 3/2)
Mol
10 mmol
PRODUCT
MOLECULE ID
JCGG-COM0001976 (Reaction Tree)
Skeleton
JCGG-STR004776
Yield
85%
REACTION DETAIL
Reaction Time
10 minutes
Reaction Temp
room temp
Solvent
pyridine + AcOH
COMMENT
Keywords: protection of sugar hydroxy groups, acyl group protection
REFERENCE
Reference Id
REF-0000-000073
Source
第4版 実験化学講座 (26), 丸善
Reference Id
REF-0000-000074
Source
ISBN 4-621-03702-1
Reference Id
REF-0000-000175
Source
H. J. Koeners, J. Verhoeven, and J. H. van Boom, Recl. Trav. Chim. Pays-Bas, 100, 65 (1981)

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)