JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001543
Submitter
The Noguchi Institute
Reaction ID
R-0000-001543
Regist Date
2012/06/21 17:19:04
REACTANT
MOLECULE ID
JCGG-COM0001971 (Reaction Tree)
Skeleton
JCGG-STR032525
Weight
1.0 g
MOLECULE ID
JCGG-COM0000838
Reactant Type
(ClCH2CO)2O
Weight
2.4 g
MOLECULE ID
JCGG-COM0000549
Reactant Type
NaHCO3
Weight
0.5 g
PRODUCT
MOLECULE ID
JCGG-COM0001972 (Reaction Tree)
Skeleton
JCGG-STR032525
Yield
85%
REACTION DETAIL
Reaction Time
2 hours
Reaction Temp
room temp
Solvent
DMF
COMMENT
Keywords: protection of sugar hydroxy groups, acyl group protection
REFERENCE
Reference Id
REF-0000-000073
Source
第4版 実験化学講座 (26), 丸善
Reference Id
REF-0000-000074
Source
ISBN 4-621-03702-1
Reference Id
REF-0000-000173
Source
G. J. F. Chittenden and H. Regeling, Recl. Trav. Chim. Pays-Bas, 106, 44 (1987)

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)