JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001542
Submitter
The Noguchi Institute
Reaction ID
R-0000-001542
Regist Date
2012/06/21 17:18:58
REACTANT
MOLECULE ID
JCGG-COM0001969 (Reaction Tree)
Skeleton
JCGG-STR031555
Mol
50 mmol
MOLECULE ID
JCGG-COM0000759
Reactant Type
imidazole
Mol
0.1 mol
MOLECULE ID
JCGG-COM0000392
Reactant Type
BzCl
Mol
50 mmol
PRODUCT
MOLECULE ID
JCGG-COM0001970 (Reaction Tree)
Skeleton
JCGG-STR031555
Yield
89% to 93%
REACTION DETAIL
Reaction Time
18 hours
Reaction Temp
reflux
Solvent
CHCl3
COMMENT
Keywords: protection of sugar hydroxy groups, acyl group protection
REFERENCE
Reference Id
REF-0000-000073
Source
第4版 実験化学講座 (26), 丸善
Reference Id
REF-0000-000074
Source
ISBN 4-621-03702-1
Reference Id
REF-0000-000172
Source
G. J. F. Chittenden, Carbohydr. Res., 16, 495 (1971)

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)