Reaction:JCGG-RAC0001519

JCGG ID

JCGG-RAC0001519

Submitter

The Noguchi Institute

Reaction ID

R-0000-001519

Regist Date

2012/06/21 17:15:58

REACTANT

MOLECULE ID

JCGG-COM0001242 (Reaction Tree)

MOLECULE ID

JCGG-COM0000043 (Reaction Tree)

Skeleton

JCGG-STR032526

MOLECULE ID

JCGG-COM0001796

Reactant Type

PhSeCl

MOLECULE ID

JCGG-COM0000625

Reactant Type

s-collidine

MOLECULE ID

JCGG-COM0001246

Reactant Type

Ph3SnH

PRODUCT

MOLECULE ID

JCGG-COM0000044 (Reaction Tree)

Yield

80%

REACTION DETAIL

Reaction Time

1 day, NOT specified

Reaction Temp

room temp, NOT specified

Solvent

MeCN, NOT specified

Comment

1) +all except Ph3SnH, 2) +Ph3SnH

Very few were described regarding this reaction.

COMMENT

Keywords: The synthesis of 2-deoxy-glycoside, glycal donor

There are multiple steps in this reaction.

REFERENCE

Reference Id

REF-0000-000073

Source

第4版実験化学講座 (26), 丸善

Reference Id

REF-0000-000074

Source

ISBN 4-621-03702-1

Reference Id

REF-0000-000161

Source

G. Jaurand, J.-M. Beau, and P. Sinay, J. Chem. Soc., Chem. Commun., 1981, 572