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Glycan Syntheses |
JCGG ID |
JCGG-RAC0001509 | ||||
Submitter |
The Noguchi Institute | ||||
Reaction ID |
R-0000-001509
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Regist Date |
2012/06/21 17:14:27 | ||||
| REACTANT | |||||
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Reactant Type |
AgOTf | ||||
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Reactant Type |
s-collidine | ||||
| PRODUCT | |||||
MOLECULE ID |
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Product Type |
alpha | ||||
Yield |
56%(alpha/beta=2/1) | ||||
MOLECULE ID |
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Product Type |
beta | ||||
Yield |
56%(alpha/beta=2/1) | ||||
| REACTION DETAIL | |||||
Reaction Time |
NOT specified | ||||
Reaction Temp |
-45 degree C to room temp | ||||
Solvent |
MeNO2, PhCH3 | ||||
Comment |
Very few were described regarding this reaction. | ||||
| MS 4A was included in the solvent. | |||||
| COMMENT | |||||
| The synthesis of 2-deoxy-glycoside, 2-deoxy-sugar donor | |||||
| ATTENTION: There is an error in the chemical structure. | |||||
| REFERENCE | |||||
Reference Id |
REF-0000-000073 | ||||
Source |
第4版 実験化学講座 (26), 丸善 | ||||
Reference Id |
REF-0000-000074 | ||||
Source |
ISBN 4-621-03702-1 | ||||
Reference Id |
REF-0000-000152 | ||||
Source |
J. Thiem and G. Schneider, Angew. Chem., Int. Ed. Engl., 22, 58 (1983) | ||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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