JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001506
Submitter
The Noguchi Institute
Reaction ID
R-0000-001506
Regist Date
2012/06/21 17:13:59
REACTANT
MOLECULE ID
JCGG-COM0001885 (Reaction Tree)
Skeleton
JCGG-STR025230
MOLECULE ID
JCGG-COM0000043 (Reaction Tree)
Skeleton
JCGG-STR032526
MOLECULE ID
JCGG-COM0000009
Reactant Type
TMSOTf
PRODUCT
MOLECULE ID
JCGG-COM0001886 (Reaction Tree)
Yield
82%
REACTION DETAIL
Reaction Time
16 hours
Reaction Temp
-35 degree C
Solvent
CH2Cl2
Comment
Very few were described regarding this reaction.
MS 5A was included in the solvent.
COMMENT
Keywords: The synthesis of 2-aminoglycoside, beta-2-aminoglycoside
REFERENCE
Reference Id
REF-0000-000073
Source
第4版 実験化学講座 (26), 丸善
Reference Id
REF-0000-000074
Source
ISBN 4-621-03702-1
Reference Id
REF-0000-000150
Source
P. Boullanger, J. Banoub, and G. Descotes, Can. J. Chem., 65, 1343 (1987)

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)