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Glycan Syntheses |
JCGG ID |
JCGG-RAC0001500 | |||||||
Submitter |
The Noguchi Institute | |||||||
Reaction ID |
R-0000-001500
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Regist Date |
2012/06/21 17:13:03 | |||||||
| REACTANT | ||||||||
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Mol |
0.77 mmol | |||||||
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Mol |
0.93 mmol | |||||||
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Reactant Type |
FeCl3 | |||||||
Weight |
185mg | |||||||
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Reactant Type |
(Me2N)2CO | |||||||
Volume |
92 micro L | |||||||
| PRODUCT | ||||||||
MOLECULE ID |
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Yield |
67% | |||||||
| REACTION DETAIL | ||||||||
Reaction Time |
overnight | |||||||
Reaction Temp |
room temp | |||||||
Solvent |
CH2Cl2 | |||||||
Comment |
anhydrous CaSO4 was included in the solvent. | |||||||
| FeCl3 and CaSO4 were mixed in CH2Cl2 and stirred for 5 to 10 minutes before the reaction. | ||||||||
| COMMENT | ||||||||
| Keywords: The synthesis of 2-aminoglycoside, beta-2-aminoglycoside | ||||||||
| REFERENCE | ||||||||
Reference Id |
REF-0000-000073 | |||||||
Source |
第4版 実験化学講座 (26), 丸善 | |||||||
Reference Id |
REF-0000-000074 | |||||||
Source |
ISBN 4-621-03702-1 | |||||||
Reference Id |
REF-0000-000146 | |||||||
Source |
M. Kiso and L. Anderson, ibid., 136, 309 (1985) | |||||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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