JCGG ID |
JCGG-RAC0001495 | ||||
Submitter |
The Noguchi Institute | ||||
Reaction ID |
R-0000-001495 | ||||
Regist Date |
2012/06/21 17:12:20 | ||||
REACTANT | |||||
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Reactant Type |
Ag2CO3 | ||||
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Reactant Type |
AgClO4 | ||||
PRODUCT | |||||
MOLECULE ID |
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Product Type |
alpha | ||||
Yield |
83%(alpha/beta=20/1) | ||||
MOLECULE ID |
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Product Type |
beta | ||||
Yield |
83%(alpha/beta=20/1) | ||||
REACTION DETAIL | |||||
Reaction Time |
NOT specified | ||||
Reaction Temp |
NOT specified | ||||
Solvent |
CH2Cl2, PhCH3 | ||||
Comment |
Very few were described regarding this reaction. | ||||
COMMENT | |||||
Keywords: The synthesis of 2-aminoglycoside, alpha-2-aminoglycoside | |||||
The reaction is the 1st part of the sequence. | |||||
ATTENTION: There is an error in the chemical structure. (HO(CH2)7CO2CH3 should be HO(CH2)8CO2CH3) | |||||
REFERENCE | |||||
Reference Id |
REF-0000-000073 | ||||
Source |
第4版 実験化学講座 (26), 丸善 | ||||
Reference Id |
REF-0000-000074 | ||||
Source |
ISBN 4-621-03702-1 | ||||
Reference Id |
REF-0000-000142 | ||||
Source |
H. Paulsen and M. Paal, Carbohydr. Res., 135, 71 (1984) |
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST) |