JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001493
Submitter
The Noguchi Institute
Reaction ID
R-0000-001493
Regist Date
2012/06/21 17:11:52
REACTANT
MOLECULE ID
JCGG-COM0001242 (Reaction Tree)
MOLECULE ID
JCGG-COM0001107
Reactant Type
CAN
MOLECULE ID
JCGG-COM0000634
Reactant Type
NaN3
MOLECULE ID
JCGG-COM0001852
Reactant Type
NaNO2
PRODUCT
MOLECULE ID
JCGG-COM0000054 (Reaction Tree)
Yield
57%
REACTION DETAIL
Reaction Time
20 hours, NOT specified
Reaction Temp
-20 degree C, 80 degree C
Solvent
MeCN, dioxane, H2O
Comment
1) +all except NaNO2, 2) +NaNO2
Very few were described regarding this reaction.
COMMENT
Keywords: The synthesis of 2-aminoglycoside, alpha-2-aminoglycoside
There are multiple steps in this reaction.
REFERENCE
Reference Id
REF-0000-000073
Source
第4版 実験化学講座 (26), 丸善
Reference Id
REF-0000-000074
Source
ISBN 4-621-03702-1
Reference Id
REF-0000-000140
Source
W. Kinzy and R. R. Schmidt, Justus Liebigs Ann. Chem., 1985, 1537

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)