JCGG ID |
JCGG-RAC0001483 | |||||||
Submitter |
The Noguchi Institute | |||||||
Reaction ID |
R-0000-001483 | |||||||
Regist Date |
2012/06/21 17:10:11 | |||||||
REACTANT | ||||||||
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Reactant Type |
SiF4 | |||||||
PRODUCT | ||||||||
MOLECULE ID |
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Product Type |
alpha | |||||||
Yield |
90%(alpha/beta=1/10) | |||||||
MOLECULE ID |
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Product Type |
beta | |||||||
Yield |
90%(alpha/beta=1/10) | |||||||
REACTION DETAIL | ||||||||
Reaction Time |
1.5 hours | |||||||
Reaction Temp |
0 degree C | |||||||
Solvent |
MeCN | |||||||
Comment |
Very few were described regarding this reaction. | |||||||
COMMENT | ||||||||
Keywords: The synthesis of 1,2-trans-glycoside, beta-glucopyranoside | ||||||||
REFERENCE | ||||||||
Reference Id |
REF-0000-000073 | |||||||
Source |
第4版 実験化学講座 (26), 丸善 | |||||||
Reference Id |
REF-0000-000074 | |||||||
Source |
ISBN 4-621-03702-1 | |||||||
Reference Id |
REF-0000-000132 | |||||||
Source |
S. Hashimoto, M. Hayashi, and R. Noyori, Tetrahedron Lett., 25, 1379 (1984) |
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST) |