JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001477
Submitter
The Noguchi Institute
Reaction ID
R-0000-001477
Regist Date
2012/06/21 17:09:15
REACTANT
MOLECULE ID
JCGG-COM0001807 (Reaction Tree)
Skeleton
JCGG-STR001961
MOLECULE ID
JCGG-COM0001808
MOLECULE ID
JCGG-COM0000009
Reactant Type
TMSOTf
PRODUCT
MOLECULE ID
JCGG-COM0001809 (Reaction Tree)
Skeleton
JCGG-STR001961
Yield
70%
REACTION DETAIL
Reaction Time
3 hours
Reaction Temp
20 degree C
Solvent
ClCH2CH2Cl
Comment
Very few were described regarding this reaction.
MS 4A was included in the solvent.
COMMENT
Keywords: The synthesis of 1,2-trans-glycoside, beta-glucopyranoside
REFERENCE
Reference Id
REF-0000-000073
Source
第4版 実験化学講座 (26), 丸善
Reference Id
REF-0000-000074
Source
ISBN 4-621-03702-1
Reference Id
REF-0000-000127
Source
T. Ogawa, K. Beppu, and S. Nakabayashi, Carbohydr. Res., 93, C6 (1981)

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)