JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001467
Submitter
The Noguchi Institute
Reaction ID
R-0000-001467
Regist Date
2012/06/21 17:07:40
REACTANT
MOLECULE ID
JCGG-COM0001782 (Reaction Tree)
MOLECULE ID
JCGG-COM0001783 (Reaction Tree)
MOLECULE ID
JCGG-COM0000032
Reactant Type
AgClO4
MOLECULE ID
JCGG-COM0000813
Reactant Type
SnCl2
PRODUCT
MOLECULE ID
JCGG-COM0001784 (Reaction Tree)
Yield
75%
REACTION DETAIL
Reaction Time
18 hours
Reaction Temp
-15 degree C
Solvent
CH2Cl2
Comment
Very few were described regarding this reaction.
MS 4A was included in the solvent.
COMMENT
Keywords: The synthesis of 1,2-trans-glycoside, beta-glucopyranoside
REFERENCE
Reference Id
REF-0000-000073
Source
第4版 実験化学講座 (26), 丸善
Reference Id
REF-0000-000074
Source
ISBN 4-621-03702-1
Reference Id
REF-0000-000119
Source
K. C. Nicolaou, J. L. Randall, and G. T. Furst, J. Am. Chem. Soc., 107, 5556 (1985)

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)