JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001461
Submitter
The Noguchi Institute
Reaction ID
R-0000-001461
Regist Date
2012/06/21 17:06:43
REACTANT
MOLECULE ID
JCGG-COM0001651 (Reaction Tree)
MOLECULE ID
JCGG-COM0001706 (Reaction Tree)
Skeleton
JCGG-STR031569
MOLECULE ID
JCGG-COM0001669
Reactant Type
Ag2O
MOLECULE ID
JCGG-COM0000084
Reactant Type
I2
PRODUCT
MOLECULE ID
JCGG-COM0001769 (Reaction Tree)
Skeleton
JCGG-STR018184
Yield
74%
REACTION DETAIL
Reaction Time
24 hours
Reaction Temp
room temp
Solvent
CHCl3
Comment
Very few were described regarding this reaction.
anhydrous CaSO4 was included in the solvent.
COMMENT
Keywords: The synthesis of 1,2-trans-glycoside, beta-glucopyranoside
REFERENCE
Reference Id
REF-0000-000073
Source
第4版 実験化学講座 (26), 丸善
Reference Id
REF-0000-000074
Source
ISBN 4-621-03702-1
Reference Id
REF-0000-000114
Source
D. D. Reynolds and W. L. Evans, J. Am. Chem. Soc., 60, 2559 (1938)

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)