JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001445
Submitter
The Noguchi Institute
Reaction ID
R-0000-001445
Regist Date
2012/06/21 17:04:00
REACTANT
MOLECULE ID
JCGG-COM0001722 (Reaction Tree)
MOLECULE ID
JCGG-COM0001723 (Reaction Tree)
Skeleton
JCGG-STR031569
MOLECULE ID
JCGG-COM0001724
Reactant Type
CuBr2
MOLECULE ID
JCGG-COM0000832
Reactant Type
Bu4NBr
PRODUCT
MOLECULE ID
JCGG-COM0001725 (Reaction Tree)
Skeleton
JCGG-STR000003
Yield
88%
REACTION DETAIL
Reaction Time
72 hours
Reaction Temp
20 degree C
Solvent
ClCH2CH2Cl, DMF
Comment
Very few were described regarding this reaction.
MS 4A was included in the solvent.
COMMENT
Keywords: The synthesis of 1,2-cis-glycoside, alpha-glucopyranoside
REFERENCE
Reference Id
REF-0000-000073
Source
第4版 実験化学講座 (26), 丸善
Reference Id
REF-0000-000074
Source
ISBN 4-621-03702-1
Reference Id
REF-0000-000100
Source
S. Sato, M. Mori, Y. Ito, and T. Ogawa, Carbohydr. Res., 155, C6 (1986)

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)