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Glycan Syntheses |
JCGG ID |
JCGG-RAC0001441 | |||||||
Submitter |
The Noguchi Institute | |||||||
Reaction ID |
R-0000-001441
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Regist Date |
2012/06/21 17:03:12 | |||||||
| REACTANT | ||||||||
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Reactant Type |
imidate | |||||||
Weight |
400mg | |||||||
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Reactant Type |
diol | |||||||
Weight |
278mg | |||||||
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Reactant Type |
p-MeC6H4SO3H (in 2 mL of MeNO2) | |||||||
Weight |
86mg | |||||||
| PRODUCT | ||||||||
MOLECULE ID |
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Yield |
71% | |||||||
| REACTION DETAIL | ||||||||
Reaction Time |
21 hours | |||||||
Reaction Temp |
room temp | |||||||
Solvent |
MeNO2 | |||||||
Comment |
Imidate, diol, and MS 4A were mixed and stirred for 3 hours before the reaction. | |||||||
| COMMENT | ||||||||
| Keywords: The synthesis of 1,2-cis-glycoside, alpha-glucopyranoside | ||||||||
| REFERENCE | ||||||||
Reference Id |
REF-0000-000073 | |||||||
Source |
第4版 実験化学講座 (26), 丸善 | |||||||
Reference Id |
REF-0000-000074 | |||||||
Source |
ISBN 4-621-03702-1 | |||||||
Reference Id |
REF-0000-000096 | |||||||
Source |
J.-C. Jacquinet, D. Duchet, M.-L. Milat, and P. Sinay, J. Chem. Soc., Perkin Trans. 1, 1981, 326. | |||||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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