JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001437
Submitter
The Noguchi Institute
Reaction ID
R-0000-001437
Regist Date
2012/06/21 17:02:22
REACTANT
MOLECULE ID
JCGG-COM0001694 (Reaction Tree)
MOLECULE ID
JCGG-COM0001695 (Reaction Tree)
Skeleton
JCGG-STR013782
MOLECULE ID
JCGG-COM0000624
Reactant Type
AgOTf
MOLECULE ID
JCGG-COM0000625
Reactant Type
2,4,6-collidine
PRODUCT
MOLECULE ID
JCGG-COM0001696 (Reaction Tree)
Skeleton
JCGG-STR020973
Yield
82%
REACTION DETAIL
Reaction Time
5 days
Reaction Temp
room temp
Solvent
CH2Cl2
Comment
Very few were described regarding this reaction.
MS 4A was included in the solvent.
COMMENT
Keywords: The synthesis of 1,2-cis-glycoside, alpha-glucopyranoside
REFERENCE
Reference Id
REF-0000-000073
Source
第4版 実験化学講座 (26), 丸善
Reference Id
REF-0000-000074
Source
ISBN 4-621-03702-1
Reference Id
REF-0000-000092
Source
H. Paulsen and O. Lockhoff, Chem. Ber., 114, 3079 (1981)

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)