JCGG ID |
JCGG-RAC0001421 | ||||
Submitter |
The Noguchi Institute | ||||
Reaction ID |
R-0000-001421 | ||||
Regist Date |
2012/06/21 17:00:18 | ||||
REACTANT | |||||
|
|
||||
Mol |
12 mmol | ||||
|
|
||||
Reactant Type |
TiBr4 | ||||
Mol |
20 mmol | ||||
PRODUCT | |||||
MOLECULE ID |
|
|
|||
Yield |
96% | ||||
REACTION DETAIL | |||||
Reaction Time |
48 hours | ||||
Reaction Temp |
room temp | ||||
Solvent |
CH2Cl2/AcOEt = 135mL/15mL | ||||
COMMENT | |||||
Keywords: The synthesis methods of glycosyl donor, glycosyl halide | |||||
REFERENCE | |||||
Reference Id |
REF-0000-000073 | ||||
Source |
第4版 実験化学講座 (26), 丸善 | ||||
Reference Id |
REF-0000-000074 | ||||
Source |
ISBN 4-621-03702-1 | ||||
Reference Id |
REF-0000-000077 | ||||
Source |
H. Paulsen and O. Lockhoff, Chem Ber., 114, 3079 (1981) |
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST) |