JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001421
Submitter
The Noguchi Institute
Reaction ID
R-0000-001421
Regist Date
2012/06/21 17:00:18
REACTANT
MOLECULE ID
JCGG-COM0001652 (Reaction Tree)
Mol
12 mmol
MOLECULE ID
JCGG-COM0001653
Reactant Type
TiBr4
Mol
20 mmol
PRODUCT
MOLECULE ID
JCGG-COM0001654 (Reaction Tree)
Yield
96%
REACTION DETAIL
Reaction Time
48 hours
Reaction Temp
room temp
Solvent
CH2Cl2/AcOEt = 135mL/15mL
COMMENT
Keywords: The synthesis methods of glycosyl donor, glycosyl halide
REFERENCE
Reference Id
REF-0000-000073
Source
第4版 実験化学講座 (26), 丸善
Reference Id
REF-0000-000074
Source
ISBN 4-621-03702-1
Reference Id
REF-0000-000077
Source
H. Paulsen and O. Lockhoff, Chem Ber., 114, 3079 (1981)

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)