JCGG ID |
JCGG-RAC0001419 | |||||||
Submitter |
The Noguchi Institute | |||||||
Reaction ID |
R-0000-001419 | |||||||
Regist Date |
2012/06/21 17:00:00 | |||||||
REACTANT | ||||||||
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|
|
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Weight |
5.65g | |||||||
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|
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Reactant Type |
HBr (30 to 32% in AcOH) | |||||||
Volume |
5.8 mL | |||||||
PRODUCT | ||||||||
MOLECULE ID |
|
|
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Yield |
90% | |||||||
REACTION DETAIL | ||||||||
Reaction Time |
2 hours | |||||||
Reaction Temp |
room temp | |||||||
Solvent |
ClCH2CH2Cl/AcOH | |||||||
COMMENT | ||||||||
Keywords: The synthesis methods of glycosyl donor, glycosyl halide | ||||||||
REFERENCE | ||||||||
Reference Id |
REF-0000-000073 | |||||||
Source |
第4版 実験化学講座 (26), 丸善 | |||||||
Reference Id |
REF-0000-000074 | |||||||
Source |
ISBN 4-621-03702-1 | |||||||
Reference Id |
REF-0000-000075 | |||||||
Source |
H. G. Fletcher, Jr., Methods Carbohydr. Chem., 2, 226 (1963) |
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST) |