JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001419
Submitter
The Noguchi Institute
Reaction ID
R-0000-001419
Regist Date
2012/06/21 17:00:00
REACTANT
MOLECULE ID
JCGG-COM0001645 (Reaction Tree)
Skeleton
JCGG-STR031555
Weight
5.65g
MOLECULE ID
JCGG-COM0001646
Reactant Type
HBr (30 to 32% in AcOH)
Volume
5.8 mL
PRODUCT
MOLECULE ID
JCGG-COM0001647 (Reaction Tree)
Yield
90%
REACTION DETAIL
Reaction Time
2 hours
Reaction Temp
room temp
Solvent
ClCH2CH2Cl/AcOH
COMMENT
Keywords: The synthesis methods of glycosyl donor, glycosyl halide
REFERENCE
Reference Id
REF-0000-000073
Source
第4版 実験化学講座 (26), 丸善
Reference Id
REF-0000-000074
Source
ISBN 4-621-03702-1
Reference Id
REF-0000-000075
Source
H. G. Fletcher, Jr., Methods Carbohydr. Chem., 2, 226 (1963)

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)