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Glycan Syntheses |
JCGG ID |
JCGG-RAC0001167 | ||||
Submitter |
The Noguchi Institute | ||||
Reaction ID |
R-0000-001164
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Regist Date |
2012/06/21 16:42:40 | ||||
| REACTANT | |||||
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Mol |
0.42 mmol | ||||
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Mol |
0.55 mmol | ||||
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Reactant Type |
Bi(OTf)3 | ||||
Mol |
0.023 mmol | ||||
| PRODUCT | |||||
MOLECULE ID |
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Yield |
81% | ||||
| REACTION DETAIL | |||||
Reaction Time |
24 hours | ||||
Reaction Temp |
0 degree C | ||||
Solvent |
CH2Cl2 | ||||
Comment |
anhydrous CaSO4 was included in the solvent. | ||||
| COMMENT | |||||
| Keywords: Crown ether, Spiroketal, 1-C-Vinylated glucose, Glycosylation | |||||
| REFERENCE | |||||
Reference Id |
REF-0000-000056 | ||||
Issn |
Electronic | ||||
PubMed ID |
18794788 | ||||
Journal Name |
Molecules (Basel, Switzerland). (2008) 13 (8): 1840-5. | ||||
Article Title |
Synthesis of a novel D-glucose-conjugated 15-crown-5 ether with a spiro ketal structure. | ||||
Author |
Takashi, Yamanoi; Yoshiki, Oda; Hitomi, Muraishi; Sho, Matsuda | ||||
Affiliation |
The Noguchi Institute, 1-8-1 Kaga, Itabashi-ku, Tokyo 173-0003, Japan. tyama@noguchi.or.jp | ||||
Reference Id |
REF-0000-000057 | ||||
Source |
Molecules 2008, 13, 1840-1845 manuscripts | ||||
Doi |
10.3390/molecules13081840 | ||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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