JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001157
Submitter
The Noguchi Institute
Reaction ID
R-0000-001166
Regist Date
2012/06/21 16:42:47
REACTANT
MOLECULE ID
JCGG-COM0001322 (Reaction Tree)
Mol
0.16 mmol
MOLECULE ID
JCGG-COM0000418
Reactant Type
NaOH (0.5 M)
Mol
2 mmol
PRODUCT
MOLECULE ID
JCGG-COM0001323 (Reaction Tree)
Yield
83%
REACTION DETAIL
Reaction Time
3 hours
Reaction Temp
room temp
Solvent
THF
COMMENT
Keywords: Crown ether, Spiroketal, 1-C-Vinylated glucose, Glycosylation
REFERENCE
Reference Id
REF-0000-000056
Issn
Electronic
PubMed ID
18794788
Journal Name
Molecules (Basel, Switzerland). (2008) 13 (8): 1840-5.
Article Title
Synthesis of a novel D-glucose-conjugated 15-crown-5 ether with a spiro ketal structure.
Author
Takashi, Yamanoi; Yoshiki, Oda; Hitomi, Muraishi; Sho, Matsuda
Affiliation
The Noguchi Institute, 1-8-1 Kaga, Itabashi-ku, Tokyo 173-0003, Japan. tyama@noguchi.or.jp
Reference Id
REF-0000-000057
Source
Molecules 2008, 13, 1840-1845 manuscripts
Doi
10.3390/molecules13081840

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)