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Glycan Syntheses |
JCGG ID |
JCGG-RAC0001118 | |||||||
Submitter |
The Noguchi Institute | |||||||
Reaction ID |
R-0000-001118
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Regist Date |
2012/06/21 16:40:04 | |||||||
| REACTANT | ||||||||
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Reactant Type |
glycal | |||||||
Mol |
1 equiv. | |||||||
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Reactant Type |
alcohol | |||||||
Mol |
1.1 equiv. | |||||||
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Reactant Type |
I(sym-collidine)2ClO4 | |||||||
Mol |
solid | |||||||
| PRODUCT | ||||||||
MOLECULE ID |
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Yield |
67% | |||||||
| REACTION DETAIL | ||||||||
Reaction Time |
1 to 2 hour(s) | |||||||
Reaction Temp |
room temp | |||||||
Solvent |
dry CH2Cl2 | |||||||
Comment |
MS 4A was included in the solvent. | |||||||
| glycal, alcohol, and MS 4A were mixed and stirred for 30 minutes at room temperature before the reaction. | ||||||||
| COMMENT | ||||||||
| The PMID could not be found. | ||||||||
| REFERENCE | ||||||||
Reference Id |
REF-0000-000051 | |||||||
Source |
J. Am. Chem. Soc., 1989, 111 (17), pp 6656-6660 | |||||||
Doi |
10.1021/ja00199a027 | |||||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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