JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001113
Submitter
The Noguchi Institute
Reaction ID
R-0000-001113
Regist Date
2012/06/21 16:39:51
REACTANT
MOLECULE ID
JCGG-COM0001242 (Reaction Tree)
Reactant Type
glycal
Mol
1 equiv.
MOLECULE ID
JCGG-COM0001243
Reactant Type
alcohol
Mol
1.1 equiv.
MOLECULE ID
JCGG-COM0000736
Reactant Type
I(sym-collidine)2ClO4
Mol
solid
PRODUCT
MOLECULE ID
JCGG-COM0001244 (Reaction Tree)
Yield
58%
REACTION DETAIL
Reaction Time
1 to 2 hour(s)
Reaction Temp
room temp
Solvent
dry CH2Cl2
Comment
MS 4A was included in the solvent.
glycal, alcohol, and MS 4A were mixed and stirred for 30 minutes at room temperature before the reaction.
COMMENT
The PMID could not be found.
REFERENCE
Reference Id
REF-0000-000051
Source
J. Am. Chem. Soc., 1989, 111 (17), pp 6656-6660
Doi
10.1021/ja00199a027

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)