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Glycan Syntheses |
JCGG ID |
JCGG-RAC0001113 | ||||
Submitter |
The Noguchi Institute | ||||
Reaction ID |
R-0000-001113
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Regist Date |
2012/06/21 16:39:51 | ||||
| REACTANT | |||||
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Reactant Type |
glycal | ||||
Mol |
1 equiv. | ||||
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Reactant Type |
alcohol | ||||
Mol |
1.1 equiv. | ||||
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Reactant Type |
I(sym-collidine)2ClO4 | ||||
Mol |
solid | ||||
| PRODUCT | |||||
MOLECULE ID |
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Yield |
58% | ||||
| REACTION DETAIL | |||||
Reaction Time |
1 to 2 hour(s) | ||||
Reaction Temp |
room temp | ||||
Solvent |
dry CH2Cl2 | ||||
Comment |
MS 4A was included in the solvent. | ||||
| glycal, alcohol, and MS 4A were mixed and stirred for 30 minutes at room temperature before the reaction. | |||||
| COMMENT | |||||
| The PMID could not be found. | |||||
| REFERENCE | |||||
Reference Id |
REF-0000-000051 | ||||
Source |
J. Am. Chem. Soc., 1989, 111 (17), pp 6656-6660 | ||||
Doi |
10.1021/ja00199a027 | ||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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