JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
 JCGG-RAC0001092
Submitter
 The Noguchi Institute
Reaction ID
 R-0000-001099
Regist Date
 2012/06/21 16:39:07
REACTANT
MOLECULE ID
 JCGG-COM0001230 (Reaction Tree)
Skeleton
JCGG-STR031375
Mol
 0.0011 mmol
MOLECULE ID
 JCGG-COM0000397
Reactant Type
 PdCl2
Mol
 0.006 mmol
PRODUCT
MOLECULE ID
 JCGG-COM0001232 (Reaction Tree)
Product Type
 alpha
Yield
 quantitative(alpha/beta=1/1)
MOLECULE ID
 JCGG-COM0001233 (Reaction Tree)
Skeleton
JCGG-STR031375
Product Type
 beta
Yield
 quantitative(alpha/beta=1/1)
REACTION DETAIL
Reaction Time
 4 hours
Reaction Temp
 room temp
Solvent
 wet MeOH
COMMENT
REFERENCE
Reference Id
 REF-0000-000048
Issn
 Print
PubMed ID
 11273599
Journal Name
 Journal of the American Chemical Society. (2001) 123 (1): 35-48.
Article Title
 Total syntheses of tumor-related antigens N3: probing the feasibility limits of the glycal assembly method.
Author
 H M, Kim; I J, Kim; S J, Danishefsky
Affiliation
 Laboratory for Bioorganic Chemistry, Sloan-Kettering Institute for Cancer Research, 1275 York Ave., New York, New York 10021, USA.
Reference Id
 REF-0000-000049
Source
 J. Am. Chem. Soc. 2001, 123, 35-48
Doi
 10.1021/ja0022730
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)