JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001047
Submitter
The Noguchi Institute
Reaction ID
R-0000-001049
Regist Date
2012/06/21 16:36:33
REACTANT
MOLECULE ID
JCGG-COM0000085 (Reaction Tree)
Reactant Type
1-C-Alkyl-glucopyranose
Mol
1.5 equiv.
MOLECULE ID
JCGG-COM0000046 (Reaction Tree)
Reactant Type
alcohol
Mol
1 equiv.
MOLECULE ID
JCGG-COM0000113
Reactant Type
Tf2NH
Mol
0.075 equiv.
PRODUCT
MOLECULE ID
JCGG-COM0000801 (Reaction Tree)
Yield
47%
REACTION DETAIL
Reaction Time
3 hours
Reaction Temp
0 degree C
Solvent
CH3CN
Comment
Drierite was included in the solvent.
COMMENT
The PMID could not be found.
ATTENTION: The chemical structure of 10a was drawn incorrectly. (compound 6 was converted from D to L)
REFERENCE
Reference Id
REF-0000-000047
Source
HETEROCYCLES, Vol. 68, No. 4, 2006. pp. 673-677
Doi
10.3987/COM-06-10684

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