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Glycan Syntheses |
JCGG ID |
JCGG-RAC0001015 | ||||
Submitter |
The Noguchi Institute | ||||
Reaction ID |
R-0000-001016
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Regist Date |
2012/06/21 16:34:46 | ||||
| REACTANT | |||||
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Reactant Type |
heptapeptide | ||||
Mol |
5.0 micro mole | ||||
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Reactant Type |
morpholine (solvent, 20% in DMF) | ||||
Volume |
1 mL | ||||
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Reactant Type |
TEA | ||||
Volume |
9 micro L | ||||
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Reactant Type |
Ac2O | ||||
Volume |
6 micro L | ||||
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Reactant Type |
DMAP | ||||
Mol |
catalytic amount | ||||
| PRODUCT | |||||
MOLECULE ID |
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Product Type |
heptapeptide acetamide | ||||
Yield |
82% | ||||
| REACTION DETAIL | |||||
Reaction Time |
60 minutes, 1 hour | ||||
Solvent |
morpholine (1 mL; 20% in DMF), CH2Cl2 (1.5 mL) | ||||
Comment |
1) heptapeptide+morpholine, 2) +all the rest | ||||
| The reaction temperature could not be found. | |||||
| COMMENT | |||||
| The PMID could not be found. | |||||
| There are two phases in this reaction. | |||||
| REFERENCE | |||||
Reference Id |
REF-0000-000046 | ||||
Source |
J. Am. Chem. Soc. 2000, 122, 7273-7279 | ||||
Doi |
10.1021/ja0011820 | ||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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