JCGG ID |
JCGG-RAC0001012 | ||||
Submitter |
The Noguchi Institute | ||||
Reaction ID |
R-0000-001013 | ||||
Regist Date |
2012/06/21 16:34:35 | ||||
REACTANT | |||||
|
|
||||
Reactant Type |
heptapeptide | ||||
Mol |
3.34 micro mole | ||||
|
|
||||
Reactant Type |
morpholine (solvent, 20% in DMF) | ||||
Volume |
1 mL | ||||
|
|
||||
Reactant Type |
TEA | ||||
Volume |
12 micro L | ||||
|
|
||||
Reactant Type |
Ac2O | ||||
Volume |
6 micro L | ||||
PRODUCT | |||||
MOLECULE ID |
|
|
|||
Product Type |
heptapeptide acetamide | ||||
Yield |
93% | ||||
REACTION DETAIL | |||||
Reaction Time |
60 minutes, 2 hours | ||||
Solvent |
morpholine (1 mL; 20% in DMF), CH2Cl2 (1 mL) | ||||
Comment |
1) heptapeptide+morpholine, 2) +all the rest | ||||
The reaction temperature could not be found. | |||||
COMMENT | |||||
The PMID could not be found. | |||||
There are two phases in this reaction. | |||||
REFERENCE | |||||
Reference Id |
REF-0000-000046 | ||||
Source |
J. Am. Chem. Soc. 2000, 122, 7273-7279 | ||||
Doi |
10.1021/ja0011820 |
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST) |