JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0001012
Submitter
The Noguchi Institute
Reaction ID
R-0000-001013
Regist Date
2012/06/21 16:34:35
REACTANT
MOLECULE ID
JCGG-COM0001137 (Reaction Tree)
Reactant Type
heptapeptide
Mol
3.34 micro mole
MOLECULE ID
JCGG-COM0001032
Reactant Type
morpholine (solvent, 20% in DMF)
Volume
1 mL
MOLECULE ID
JCGG-COM0000047
Reactant Type
TEA
Volume
12 micro L
MOLECULE ID
JCGG-COM0000086
Reactant Type
Ac2O
Volume
6 micro L
PRODUCT
MOLECULE ID
JCGG-COM0001138 (Reaction Tree)
Product Type
heptapeptide acetamide
Yield
93%
REACTION DETAIL
Reaction Time
60 minutes, 2 hours
Solvent
morpholine (1 mL; 20% in DMF), CH2Cl2 (1 mL)
Comment
1) heptapeptide+morpholine, 2) +all the rest
The reaction temperature could not be found.
COMMENT
The PMID could not be found.
There are two phases in this reaction.
REFERENCE
Reference Id
REF-0000-000046
Source
J. Am. Chem. Soc. 2000, 122, 7273-7279
Doi
10.1021/ja0011820

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)