JCGG ID |
JCGG-RAC0000995 | |||||||
Submitter |
The Noguchi Institute | |||||||
Reaction ID |
R-0000-000996 | |||||||
Regist Date |
2012/06/21 16:33:40 | |||||||
REACTANT | ||||||||
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Mol |
0.104 mmol | |||||||
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Mol |
0.208 mmol | |||||||
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Reactant Type |
NIS | |||||||
Mol |
0.260 mmol | |||||||
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Reactant Type |
TfOH (1% in CH2Cl2) | |||||||
Mol |
0.104 mmol | |||||||
PRODUCT | ||||||||
MOLECULE ID |
|
|
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Yield |
82% | |||||||
REACTION DETAIL | ||||||||
Reaction Time |
30 minutes, 30 minutes | |||||||
Reaction Temp |
room temp, 0 degree C | |||||||
Solvent |
CH2Cl2, CH2Cl2 | |||||||
Comment |
1) 22+19, MS 4A, 2) +all the rest | |||||||
MS 4A was included in the solvent. | ||||||||
COMMENT | ||||||||
The PMID could not be found. | ||||||||
There are two phases in this reaction. | ||||||||
REFERENCE | ||||||||
Reference Id |
REF-0000-000046 | |||||||
Source |
J. Am. Chem. Soc. 2000, 122, 7273-7279 | |||||||
Doi |
10.1021/ja0011820 |
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST) |