JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0000995
Submitter
The Noguchi Institute
Reaction ID
R-0000-000996
Regist Date
2012/06/21 16:33:40
REACTANT
MOLECULE ID
JCGG-COM0001018 (Reaction Tree)
Skeleton
JCGG-STR025660
Mol
0.104 mmol
MOLECULE ID
JCGG-COM0001121 (Reaction Tree)
Mol
0.208 mmol
MOLECULE ID
JCGG-COM0000129
Reactant Type
NIS
Mol
0.260 mmol
MOLECULE ID
JCGG-COM0000111
Reactant Type
TfOH (1% in CH2Cl2)
Mol
0.104 mmol
PRODUCT
MOLECULE ID
JCGG-COM0001122 (Reaction Tree)
Yield
82%
REACTION DETAIL
Reaction Time
30 minutes, 30 minutes
Reaction Temp
room temp, 0 degree C
Solvent
CH2Cl2, CH2Cl2
Comment
1) 22+19, MS 4A, 2) +all the rest
MS 4A was included in the solvent.
COMMENT
The PMID could not be found.
There are two phases in this reaction.
REFERENCE
Reference Id
REF-0000-000046
Source
J. Am. Chem. Soc. 2000, 122, 7273-7279
Doi
10.1021/ja0011820

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)