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Glycan Syntheses |
JCGG ID |
JCGG-RAC0000985 | ||||
Submitter |
The Noguchi Institute | ||||
Reaction ID |
R-0000-000985
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Regist Date |
2012/06/21 16:33:08 | ||||
| REACTANT | |||||
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Mol |
73.1 micro mole | ||||
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Reactant Type |
Cl3CCN | ||||
Mol |
7.31 mmol | ||||
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Reactant Type |
K2CO3 | ||||
Mol |
3.66 mmol | ||||
| PRODUCT | |||||
MOLECULE ID |
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Product Type |
alpha | ||||
Yield |
89%(alpha/beta=1/2) | ||||
MOLECULE ID |
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Product Type |
beta | ||||
Yield |
89%(alpha/beta=1/2) | ||||
| REACTION DETAIL | |||||
Reaction Time |
8 hours | ||||
Reaction Temp |
room temp | ||||
Solvent |
CH2Cl2 | ||||
Comment |
The reactants were mixed at 0 degree in Celsius before stirred at room temperature. | ||||
| COMMENT | |||||
| The PMID could not be found. | |||||
| REFERENCE | |||||
Reference Id |
REF-0000-000046 | ||||
Source |
J. Am. Chem. Soc. 2000, 122, 7273-7279 | ||||
Doi |
10.1021/ja0011820 | ||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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