|
Glycan Syntheses |
JCGG ID |
JCGG-RAC0000971 | |||||||
Submitter |
The Noguchi Institute | |||||||
Reaction ID |
R-0000-000971
|
|||||||
Regist Date |
2012/06/21 16:32:24 | |||||||
| REACTANT | ||||||||
|
|
|
|
||||||
Mol |
11.42 mmol | |||||||
|
|
|
|||||||
Reactant Type |
MeC(OMe)3 | |||||||
Volume |
3.5 mL | |||||||
|
|
|
|||||||
Reactant Type |
PTS | |||||||
Mol |
catalytic quantity | |||||||
|
|
|
|||||||
Reactant Type |
AcOH (80%) | |||||||
Volume |
165 mL | |||||||
| PRODUCT | ||||||||
MOLECULE ID |
|
|
|
|||||
Yield |
90% | |||||||
| REACTION DETAIL | ||||||||
Reaction Time |
10 minutes, 15 minutes | |||||||
Solvent |
CH3CN, CH3CN/AcOH | |||||||
Catalyst |
PTS (first phase) | |||||||
Comment |
1) 22+MeC(OMe)3, PTS, 2) +AcOH | |||||||
| The reaction temperature could not be found. (considered to be room temp) | ||||||||
| COMMENT | ||||||||
| The PMID could not be found. | ||||||||
| There are two phases in this reaction. | ||||||||
| REFERENCE | ||||||||
Reference Id |
REF-0000-000044 | |||||||
Source |
Journal of Carbohydrate Chemistry, 17: 4, 739-758 | |||||||
Doi |
10.1080/07328309808002349 | |||||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
|
