JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0000957
Submitter
The Noguchi Institute
Reaction ID
R-0000-000957
Regist Date
2012/06/21 16:31:44
REACTANT
MOLECULE ID
JCGG-COM0001083 (Reaction Tree)
Skeleton
JCGG-STR025539
Mol
7.79 mmol
MOLECULE ID
JCGG-COM0001081 (Reaction Tree)
Skeleton
JCGG-STR032134
Reactant Type
(in 100 mL of CH2Cl2)
Mol
31.18 mmol
MOLECULE ID
JCGG-COM0000009
Reactant Type
TMSOTf (0.01 M in CH2Cl2)
Mol
0.078 mmol
PRODUCT
MOLECULE ID
JCGG-COM0001088 (Reaction Tree)
Skeleton
JCGG-STR026714
Yield
90%
REACTION DETAIL
Reaction Time
5 minutes
Reaction Temp
0 degree C
Solvent
dry CH2Cl2
Comment
6 was added slowly.
COMMENT
The PMID could not be found.
REFERENCE
Reference Id
REF-0000-000044
Source
Journal of Carbohydrate Chemistry, 17: 4, 739-758
Doi
10.1080/07328309808002349

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)